刘永涛, 沈丹怡, 董靖, 杨秋红, 杨移斌, 周顺, 艾晓辉. Determination of Niclosamide in Water,Sediment,Fish and Shrimp by HPLC-MS/MS Method with Isotope Dilution[J]. 2020, 39(8): 980-985.
DOI:
刘永涛, 沈丹怡, 董靖, 杨秋红, 杨移斌, 周顺, 艾晓辉. Determination of Niclosamide in Water,Sediment,Fish and Shrimp by HPLC-MS/MS Method with Isotope Dilution[J]. 2020, 39(8): 980-985.DOI: doi:10.3969/j.issn.1004-4957.2020.08.006.
Determination of Niclosamide in Water,Sediment,Fish and Shrimp by HPLC-MS/MS Method with Isotope Dilution
A high performance liquid chromatography-tandem mass spectrometry(HPLC-MS/MS) with isotope dilution was established for the determination of niclosamide(NIC) in water
sediment
fish muscle and skin in natural proportions and shrimp muscle.The water sample was extracted with ethyl acetate after alkalization treatment
and the other samples were extracted with acetonitrile containing 0.1% ammonia
and purified using C18 powder.The extracts were separated on a Thermo Hypersil Gold C18(150 mm×2.1 mm,5 μm) column with acetonitrile-water as mobile phase at a flow rate of 0.3 mL/min
then detected in selected reaction monitoring(SRM) mode and quantified by internal standard calibration curve method with the stable isotope marker of NIC(NIC-13C6) as internal standard.Results showed that good linearities for NIC in the samples were observed in the range of 0.2-200 μg/L
with their correlation coefficients(r2) not less than 0.999 5.The average recoveries for NIC in water at three spiked levels of 2.5
25 and 250 ng/L ranged from 90.5% to 109% with relative standard deviations(RSD) of 3.2%-11%.The limit of detection(LOD) and limit of quantitation(LOQ) for NIC in water were 1.0 ng/L and 2.5 ng/L
respectively.While for NIC in sediment
fish muscle and skin in natural proportions and Procambarus clarkii muscle
the average recoveries at three spiked levels of 0.5
5.0 and 50 μg/kg were in the ranges of 89.4%-113%
92.8%-110% and 94.1%-107%
with their RSDs of 46%-12%
2.8%-11% and 3.2%-9.3%
respectively.The LODs and LOQs were 0.2 μg/kg and 0.5 μg/kg
respectively.With high sensitivity
accuracy and selectivity
the present method is suitable for the determination of NIC residues in practical aquatic environmental water
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Related Author
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Related Institution
中国水产科学研究院珠江水产研究所
哈尔滨工业大学 理学院
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