Detection of Volatile Compounds in Edible Birds Nest by Using Solid Phase Micro-extraction/Gas Chromatography-Mass Spectrometry

柳训才; 张小江; 张晓婷; 徐敦明; 范群艳

doi:doi：10.3969/j.issn.1004-4957.2020.02.006

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Detection of Volatile Compounds in Edible Birds Nest by Using Solid Phase Micro-extraction/Gas Chromatography-Mass Spectrometry

更新时间：2023-05-25

- Detection of Volatile Compounds in Edible Birds Nest by Using Solid Phase Micro-extraction/Gas Chromatography-Mass Spectrometry
- Vol. 39, Issue 2, Pages: 205-211(2020)
- 作者机构：
  
  1. 燕之屋丝浓食品有限公司燕窝技术中心
  2. 厦门海关检验检疫技术中心
- 作者简介：
- 基金信息：
- DOI：doi：10.3969/j.issn.1004-4957.2020.02.006
  CLC：
- Published：2020
- 稿件说明：
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柳训才, 张小江, 张晓婷, 徐敦明, 范群艳. Detection of Volatile Compounds in Edible Birds Nest by Using Solid Phase Micro-extraction/Gas Chromatography-Mass Spectrometry[J]. 2020, 39(2): 205-211.
DOI：

柳训才, 张小江, 张晓婷, 徐敦明, 范群艳. Detection of Volatile Compounds in Edible Birds Nest by Using Solid Phase Micro-extraction/Gas Chromatography-Mass Spectrometry[J]. 2020, 39(2): 205-211. DOI： doi：10.3969/j.issn.1004-4957.2020.02.006.

摘要

该文以印尼产的燕窝为材料，使用固相微萃取(SPME)技术萃取燕窝中挥发性成分并以气相色谱-质谱(GC-MS)联用仪进行测定。考察了萃取头类型、萃取温度、萃取时间和解吸时间对固相微萃取(SPME)在燕窝挥发性成分测定中的影响。结果表明：以65 μm聚二甲基硅氧烷/二乙烯基苯(PDMS/DVB)萃取头、在60 ℃下萃取60 min，解吸2 min的条件下，SPME/GC-MS技术可检出燕窝中挥发性成分醇、烃、醛、酯、醚类等化合物共82种。该方法具有操作简便、快速、重复性好和灵敏度高的特点，适用于燕窝中挥发性成分的测定。

Abstract

A solid phase micro extraction(SPME)/gas chromatography-mass spectrometry(GC-MS) was established for the detection of volatile compounds in edible bird's nest(EBN) derived from Indonesia.The samples were extracted by SPME and identified by GC-MS.Effects of type of SPME column

extraction time

extraction temperature and desorbing time on extraction efficiencies for volatile compounds in EBN were investigated.Results indicated that 82 kinds of alcohols

hydrocarbons

aldehydes

esters

ethers

and etc.in EBN were detected with a 65 μm polydimethylsiloxane/divinylbenzene(PDMS/DVB) fused silica fiber at 60 ℃ for extraction time of 60 min and desorbing time of 2 min.With the characteristics of easy operation

rapidness

high repeatability and high sensitivity

the method is suitable for determination of the volatile compounds in EBN.

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