Analysis of Differences in Volatile Flavor Components of Cigarette Breakable Capsules Based on HS-GC-IMS

JIN Qiang; SUN Xue-feng; TANG Wei; HU Yu-xuan; LUO Liang; LU Fei; LIAO Hui-yun

doi:10.12452/j.fxcsxb.23110102

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Analysis of Differences in Volatile Flavor Components of Cigarette Breakable Capsules Based on HS-GC-IMS

Scientific Papers | 更新时间：2024-04-18

- Analysis of Differences in Volatile Flavor Components of Cigarette Breakable Capsules Based on HS-GC-IMS
- Journal of Instrumental Analysis Vol. 43, Issue 4, Pages: 574-581(2024)
- 作者机构：
  
  1.南通烟滤嘴有限责任公司，江苏南通 226014
  2.江苏中烟工业有限责任公司，江苏南京 210019
- 作者简介：
- 基金信息：
- DOI：10.12452/j.fxcsxb.23110102
  CLC： O657.7;TS41.1
- Published：15 April 2024，
  
  Received：01 November 2023，
  
  Revised：14 January 2024，
- 稿件说明：
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金强,孙学锋,唐伟等.基于HS-GC-IMS分析爆珠香精挥发性风味成分差异[J].分析测试学报,2024,43(04):574-581.

JIN Qiang,SUN Xue-feng,TANG Wei,et al.Analysis of Differences in Volatile Flavor Components of Cigarette Breakable Capsules Based on HS-GC-IMS[J].Journal of Instrumental Analysis,2024,43(04):574-581.
金强,孙学锋,唐伟等.基于HS-GC-IMS分析爆珠香精挥发性风味成分差异[J].分析测试学报,2024,43(04):574-581. DOI： 10.12452/j.fxcsxb.23110102.

JIN Qiang,SUN Xue-feng,TANG Wei,et al.Analysis of Differences in Volatile Flavor Components of Cigarette Breakable Capsules Based on HS-GC-IMS[J].Journal of Instrumental Analysis,2024,43(04):574-581. DOI： 10.12452/j.fxcsxb.23110102.

摘要

采用顶空气相色谱-离子迁移谱（HS-GC-IMS）技术，对不同清新玫瑰爆珠样品中的香精挥发性成分进行鉴定，并通过感官评价，结合主成分分析（PCA）、偏最小二乘判别分析（PLS-DA）、偏最小二乘回归法（PLSR）等多元统计方法识别判定不同样品的主要风味成分差异。结果表明：①感官评价显示该爆珠样品风格特征主要以花香、果香、木香为主，并辅以青香、甜香与酒香香韵，不同样品在花香、果香属性上呈显著差异（

0.05）；②GC-IMS非靶向定性出样品中22种主要的挥发性风味组分，其中醇类8种、酯类3种、酮类3种、醛类3种、烯烃类3种、酸类1种、吡嗪类1种，且指纹图谱直观显示出挥发性较强的醇类、酯类等香气化合物在样品间差异明显；③PCA、PLS-DA能对不同样品进行有效区别，并筛选出10个特征差异组分（VIP

1），PLSR得出样品感官差异主要与2-甲基丁酸乙酯、丁酸乙酯、环己酮、苯乙酮、辛醛、正丙醇和芳樟醇有关。该方法可有效区分不同清新玫瑰爆珠样品，其判定结果与感官评价结果一致，具有准确可靠、可视化强等特点，能够为烟用爆珠产品感官质量快速检验提供技术支持。

Abstract

A headspace gas chromatography-ion migration spectrometry（HS-GC-IMS） was used to identify the volatile components in different fresh rose breakable capsules samples. The sensory evaluation combined with principal component analysis（PCA），partial least squares discriminant analysis（PLS-DA），partial least squares regression（PLSR） and other multivariate statistical methods were used to identify the differences of major flavor components in different samples. The results showed as follows：①The sensory evaluation showed that the flavor characteristics of the breakable capsules samples were mainly floral，fruity and woody，supplemented by green，sweet and wine aromas. The floral and fruity characteristics of different samples showed significant differences（

0.05）. ②The 22 main volatile flavor components in the samples were identified by GG-IMS，including 8 alcohols，3 esters，3 ketones，3 aldehydes，3 olefins，1 acids and 1 pyazines. The fingerprint directly showed that the aroma compounds with strong volatility，such as alcohols and esters，were significantly different among the samples. ③PCA and PLS-DA can effectively distinguish different samples and screen out 10 characteristic difference components（VIP

1）. PLSR showed that the sensory differences of samples were mainly related to ethyl 2-methylbutyrate，ethyl butyrate，cyclohexanone，acetophenone，octanal，

-propanol and linalool. The method can effectively distinguish different fresh rose breakable capsules samples，and its determination results are consistent with the results of sensory evaluation. It has the characteristics of accuracy，reliability，strong visualization，etc.，and can provide technical support for rapid inspection of sensory quality of cigarette breakable capsules products.

关键词

烟草爆珠气相色谱-离子迁移谱风味分析

Keywords

tobaccobreakable capsulesGC-IMSflavoranalysis

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