A solid-phase extraction and capillary gas chromatographic method was developed for the determination of BHC & DDT pesticide residues in cinnamomum cassia bark.The pesticide residues were extracted by vortex oscillation using acetone-petroleum ether mixed solvent as extraction agent,and the extract was purified by solid-phase extraction technology.The proportion and dosage of the elution solvent were optimized,and the detection of targeted compounds was performed by GC/μECD.Under the optimal conditions,the calibration curves were linear in the range of 10-1 000 μg/L ,with correlations coefficients of 0.995 8-0.998 1.The average recoveries for BHC and DDT were in the range of 92.1%-112% with RSDs（n=5） of 2.8%-8.1%.The limits of detection（LODs） were 5.0×10-3-2.4×10-2 mg?kg-1，and the limits of quantitations（LOQs） were 1.3×10-2-6.0×10-2 mg?kg-1.The method was simple，sensitive,accurate and reproducible.