A method for the determination of 5 chlorophenols（PCPs） and o-phenyphenol（OPP） in textiles using dispersive liquid-liquid microextraction（DLLME）coupled with gas chromatography-mass spectrometry（GC-MS） was proposed.Some important parameters affecting extraction efficiency，such as kind of extraction and dispersed solvents and their volume，concentration of K2CO3 were investigated.The optimal conditions were as follows：the sample was extracted with 0.15 mol/L K2CO3 solution in ultrasonic bath.Then 5 mL solution was derivatized with 0.1 mL acetic anhydride for 2 min，then extracted with 0.6 mL of isopropanol（as dispersive solvent） and 0.2 mL carbon tetrachloride （as extraction solution） in ultrasonic bath for 3 min，centrifuged for 3 min at a rate of 4 000 r/min.The lower organic phase was injected to analyze by GC-MS.Under the optimum conditions，the calibration curves were linear in the range of 0.001-1 mg/L，with correlation coefficients of 0.999 1-0.999 9.The detection limits（S/N=3） were in the range of 0.5-5 μg/kg.The average recoveries of the spiked samples were in the range of 87.2%-103.7% with relative standard deviations of 2.5%-4.8%.With the advantages of convinience，sensitivity，good recovery and repeatability，the method was suitable for the detection of 5 chlorophenols and o-phenyphenol in textile samples.