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1.重庆市食品药品检验检测研究院,重庆 400030
2.国家市场监管重点实验室(调味品监管技术), 重庆 400030
Published:15 December 2024,
Received:25 April 2024,
Revised:01 July 2024,
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冯桂蓉,李红,黄先亮,黄丹丹,陈力维,蔡小钦,黄思瑜,侯美玲.基于色谱技术的食品中多环芳烃检测方法研究进展[J].分析测试学报,2024,43(12):2031-2042.
FENG Gui-rong,LI Hong,HUANG Xian-liang,HUANG Dan-dan,CHEN Li-wei,CAI Xiao-qin,HUANG Si-yu,HOU Mei-ling.Advance in Chromatographic Techniques for Polycyclic Aromatic Hydrocarbons Detection in Food[J].Journal of Instrumental Analysis,2024,43(12):2031-2042.
冯桂蓉,李红,黄先亮,黄丹丹,陈力维,蔡小钦,黄思瑜,侯美玲.基于色谱技术的食品中多环芳烃检测方法研究进展[J].分析测试学报,2024,43(12):2031-2042. DOI: 10.12452/j.fxcsxb.24042501.
FENG Gui-rong,LI Hong,HUANG Xian-liang,HUANG Dan-dan,CHEN Li-wei,CAI Xiao-qin,HUANG Si-yu,HOU Mei-ling.Advance in Chromatographic Techniques for Polycyclic Aromatic Hydrocarbons Detection in Food[J].Journal of Instrumental Analysis,2024,43(12):2031-2042. DOI: 10.12452/j.fxcsxb.24042501.
多环芳烃(PAHs)是一类持久性有机污染物,广泛存在于多种食品中,严重危害人体健康。色谱法为检测食品中PAHs的主要方法。但由于食品类型多样且基质复杂,PAHs组分较多且化学性质各异,建立适用于多类型食品的前处理及色谱方法具有挑战。该文综述了利用色谱方法检测食品中PAHs的近期研究进展,归纳了液液萃取法、固相萃取法、快速同时萃取法等多种常用的前处理方法,梳理了高效液相色谱、气相色谱及与质谱联用等常用色谱法的应用,并对前处理及色谱方法的优势和不足进行了系统总结。对于不同类型食品,如畜禽肉类、食用油、乳及乳制品等,梳理了其主要的前处理技术和色谱检测方法,并对前处理和色谱技术的研究趋势进行了展望,旨在为开发不同食品类型中多组分PAHs的色谱检测方法提供理论支撑。
Polycyclic aromatic hydrocarbons(PAHs) are a class of persistent organic pollutants,which are widely present in various foods and seriously danger to human health. The primary detection method is chromatography. However,it is challenging to investigate appropriate pre-treatment and chromatography methods for different types of food,due to the diversity of food types,the complexity of food matrices,and the numerous and chemically diverse components of PAHs. This review summarized recent research progress in detection of PAHs in foods by chromatography. It summarized commonly used pre-treatment methods,including liquid-liquid extraction(LLE),solid-phase extraction and quick(SPE),easy,cheap,effective,rugged and safe extraction(QuEChERS) and so on. Additionally,it outlined the applications of common chromatographic methods such as high-performance liquid chromatography(HPLC),gas chromatography and combination with mass spectrometry(GC-MS). In addition,the advantages and limitations of these pre-treatment and chromatographic methods were systematically summarized. For different types of foods,such as livestock and poultry meat,edible oils,and dairy products,the primary pre-treatment techniques and chromatographic detection methods were presented. In this article,it also provided an outlook on the research trends in pre-treatment and chromatographic techniques. This review aims to offer theoretical support for the development of chromatographic detection methods for multi-component PAHs in various food types,further promotes the improvement of detection methods and establish limit standards systems for PAHs in different types of food in China.
食品多环芳烃前处理方法色谱方法
foodpolycyclic aromatic hydrocarbons(PAHs)pre-treatment methodchromatographic method
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