A method of supercritical CO2 fluid extraction gas chromatography-mass spectrometry (GC-MS) was developed for the determination of fragrance allergens in toy material.The optimal conditions were as follows:extraction temperature:50 ℃,pressure:300 bar;carbon dioxide flow rate:30 g/min; content of methanol entrainer:3%,dynamic extraction:30 min;static extraction time:30 min.Under the optimal conditions,the extracts were separated on a DB-17MS column,then determined by GC-MS and quantified by the internal standard method.The calibration curves were linear in the range of 0.02-60 μg/mL with correlation coefficients of 0.993 2-0.999 9 and detection limits(S/N=10) of 0.02-0.09 μg/mL.The average recoveries of the target compounds in polypropylene(PP),polyethylene(PE),alkyl benzo sulfonate(ABS) plastic samples were in the ranges of 79.6%-114.5%,75.0%-118.9% and 72.7%-114.9%，respectively.The relative standard deviations were in the ranges of 3.2%-11.0%,0.6%-11.6%,3.5%-11.0%.The results showed that this method was sensitive,reliable and environmental for the qualitative and quantitative determinations of fragrance allergens in toy product.