Determination of 31 Organophosphorous Pesticide Residues in Fruits by Gas Chromatography with QuEChERS Sample Preparation
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Determination of 31 Organophosphorous Pesticide Residues in Fruits by Gas Chromatography with QuEChERS Sample Preparation
Vol. 35, Issue 8, Pages: 1021-1025(2016)
作者机构:
1. 中国农业科学院果树研究所
2. 农业部果品质量安全风险评估实验室(兴城)
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Determination of 31 Organophosphorous Pesticide Residues in Fruits by Gas Chromatography with QuEChERS Sample Preparation. [J]. 35(8):1021-1025(2016)
DOI:
Determination of 31 Organophosphorous Pesticide Residues in Fruits by Gas Chromatography with QuEChERS Sample Preparation. [J]. 35(8):1021-1025(2016)DOI:
Determination of 31 Organophosphorous Pesticide Residues in Fruits by Gas Chromatography with QuEChERS Sample Preparation
A method of QuEChERS sample preparation was optimized and the QuEChERS-GC method for simultaneous analysis of 31 organophosphorous pesticide residues in fruits were established in this study.The samples were extracted with acetonitrile,and salted out with sodium chloride.The extracts were cleaned up by dispersive solid phase extraction using C18 and magnesium sulfate as sorbents,then determined by GC/FPD with matrix-matched standards procedure.The external standard method was used for quantitative analysis.The results showed that the correlation coefficients of linear equations(r2) were in the range of 0.990 3-0.999 9.The recoveries of 31 organophosphorus pesticides in various spiked levels ranged from 81.7% to 120.7%,with RSDs of 0.4%-14.7%.The limits of detection(LOD) were in the range of 0.4-6 μg?kg-1.The method showed the advantages of simplicity,rapidness,sensitivity and low consumption.It could meet the demands for the simultaneous determination of multi-residue organophosphorous pesticides in fruits.
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Evaluation of QuEChERS Method for the Analysis of 15 Triazole Pesticides Residues in Fruits by Online Gel Permeation Chromatography Gas Chromatography-Mass Spectrometry
Residue Determination of Niclosamide-olamine in Twenty Two Kinds of Agricultural Products by UPLC-MS/MS
Simultaneous Determination of 16 Coumarins and Vanillins and Their Derivatives in Rice by QuEChERS-Isotope Internal Standard/Ultra-high Performance Liquid Chromatography-Tandem Mass Spectrometry
Screening of 166 Pesticide Residues in Tea Based on Ultra High Performance Liquid Chromatography-Quadrupole/Electrostatic Field Orbitrap High Resolution Mass Spectrometry
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NHC Key Laboratory of Food Safety Risk Assessment, China National Center for Food Safety Risk Assessment