Determination of Tetracyclines Residues in Pork by High Performance Liquid Chromatography-Tandem Mass Spectrometry with Modified QuEChERS Sample Pretreatment
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Determination of Tetracyclines Residues in Pork by High Performance Liquid Chromatography-Tandem Mass Spectrometry with Modified QuEChERS Sample Pretreatment
Vol. 36, Issue 2, Pages: 272-275(2017)
作者机构:
1. 天津出入境检验检疫局动植物与食品检测中心
2. 安捷伦科技有限公司
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Determination of Tetracyclines Residues in Pork by High Performance Liquid Chromatography-Tandem Mass Spectrometry with Modified QuEChERS Sample Pretreatment. [J]. 36(2):272-275(2017)
DOI:
Determination of Tetracyclines Residues in Pork by High Performance Liquid Chromatography-Tandem Mass Spectrometry with Modified QuEChERS Sample Pretreatment. [J]. 36(2):272-275(2017)DOI:
Determination of Tetracyclines Residues in Pork by High Performance Liquid Chromatography-Tandem Mass Spectrometry with Modified QuEChERS Sample Pretreatment
A modified QuEChERS sample pretreatment method was established for the determination of tetracycline residues in pork.The new method adopted a novel lipid-removal material(EMR-Lipid) in QuEChERS procedure,and provided fast and effective sample extraction and cleanup of high-fat sample such as pork.The LODs of the method were 5.0 μg/kg.The recoveries of tetracycline,chlortetracycline,doxycycline were in the range of 75.6%-89.4% and the recoveries of oxytetracycline were in the range of 53.4%-61.0%,with RSDs not more than 7.7%.
关键词
EMR-LipidQuEChERS四环素类兽药残留高效液相色谱-串联质谱
Keywords
EMR-LipidQuEChERStetracyclinesresidue detectionhigh performance liquid chromatography-tandem mass spectrometry(HPLC-MS/MS)
Determination of Malachite Green,Crystal Violet and Their Metabolites Residues in Aquatic Product by QuEChERS Combined with UPLC-MS/MS
Determination of Thiacloprid,Spirotetramat and Its Metabolites Residues in Litchi and Longan by High Performance Liquid Chromatography-Tandem Mass Spectrometry
Residue Determination of Niclosamide-olamine in Twenty Two Kinds of Agricultural Products by UPLC-MS/MS
Simultaneous Determination of 16 Coumarins and Vanillins and Their Derivatives in Rice by QuEChERS-Isotope Internal Standard/Ultra-high Performance Liquid Chromatography-Tandem Mass Spectrometry
Screening of 166 Pesticide Residues in Tea Based on Ultra High Performance Liquid Chromatography-Quadrupole/Electrostatic Field Orbitrap High Resolution Mass Spectrometry
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潍坊出入境检验检疫局
广东省农业科学院植物保护研究所广东省植物保护新技术重点实验室
广东检验检疫技术中心
College of Horticulture and Landscape,Tianjin Agricultural University
Hainan Provincial Key Laboratory of Quality and Safety for Tropical Fruits and Vegetables;Key Laboratory of Quality and Safety Control for Subtropical Fruit and Vegetable,Ministry of Agriculture and Rural Affairs;Analysis and Test Center,Chinese Academy of Tropical Agricultural Sciences