A method was developed for the simultaneous determination of 19 chlorinated phenols in textiles by liquid chromatography-mass spectrometry(LC-MS).The textile samples were extracted with methanol in ultrasonic bath,then evaporated and set to volume.The target compounds were analyzed by LC-MS and quantified by the external method.The calibration curves for 19 chlorinated phenols were linear(r>0.999 90) in the concentration range of 0.05-5.0 mg/L.The average recoveries were in the range of 80.3%-104% with their relative standard deviations(RSD,n=6) of 4.0%-9.8%.The quantitation limits were 0.05 mg/kg.The method was sensitive,simple,efficient and accurate,and could meet the requirements for detection of chlorinated phenols in textile products.
Simultaneous and Rapid Determination of 102 Acidic,Alkaline and Neutral Organic Pollutants in Groundwater by Gas Chromatography-Mass Spectrometry
Determination of Organic Halides in Textiles by Ion Chromatography Method with High Temperature Combustion and Water Vapor Absorption
Determination of Quinoline and Isoquinoline in Textiles by Gas Chromatography-Mass Spectrometry
Simultaneous Determination of 65 Polychlorinated Biphenyls,Polycyclic Aromatic Hydrocarbons and Organochlorine Pesticides in Marine Sediments by GC-MS with Accelerated Solvent Extraction
Simultaneous Determination of Six Effective Components in Lianhuaqingwen Capsule by Micellar Electrokinetic Capillary Chromatography
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